Micro-deposition Improves Analysis

DiscovIR’s unique temperature controlled, vacuum deposition method ensures that results are accurate and reproducible. Eluted peaks are first deposited in a film on to a rotating IR transparent disc. Next, an infrared beam passes through each concentrated spot and the detector automatically collects spectral data.

Concentrates Analytes In Minimal Area

Cryogenic temperature control of the Sample Disc minimizes the area of the deposited analyte. This results in a thicker sample layer and therefore Higher Sensitivity of the absorbance spectrum.

New DiscovIR-LCTM system from Spectra Analysis is able to afford total solvent removal from a reversed-phase gradient run (2% to 100% organic) with no change in the operational setpoints of the system. Solid phase Transmission FTIR Spectra are acquired continuously throughout the run.

Key Applications

• Deformulation
• Co-polymer compositional drift
• Extractables and leachables
• Minor component identification
• Chemical troubleshooting
• Degradation/failure analysis

For all laboratory applications even for sophisticated state-of-the-art sterilization processes.

With all possibilities to add additional options for process optimization to enable validatable sterilization to be carried out.

Dilatometry measures the change in size of a sample as a function of temperature. In addition to directly determining the thermal expansion of the sample, the change in size also provides information about phase transitions and physical or chemical changes in the microstructure. These can be identified by the associated changes in density and rate of expansion of the material. Dilatometry is also an extremely useful method for evaluating the sintering behavior of materials, as it records both the shrinkage of a sintered sample and the temperatures required to achieve this change. This analysis allows optimization of workpiece shapes and processing temperatures, improvement of product quality and reduction of costs.

Key Features

• Patented, linear motor and high-resolution displacement sensor provide unmatched control over the widest ranges of force, displacement, and frequency, for superior data accuracy
• Ultra-durable, frictionless motor, backed by the industry’s only ten-year warranty, provides maintenance- and worry-free operation
• High force of 500 N enables testing of larger samples or final parts under real-world conditions, by achieving higher loading levels in both DMA and fatigue analysis
• Forced Convection Oven (FCO) provides superior control and responsiveness over a temperature range of -150 °C to 600 °C for the highest degree of accuracy and flexibility in experiment thermal profiles
• Large Sample Oven (LSO), with a temperature range of -150 °C to 315 °C, offers spacious interior dimensions to accommodate testing of large samples or component
• Air Chiller Systems (ACS) offer unique gas flow cooling for sub-ambient testing without the use of liquid nitrogen, eliminating potential laboratory hazards while providing an incredible return on investment
• Broad range of fixtures accommodate a wide range of sample sizes and geometries adding to testing versatility
• Extremely rigid test frame and air bearings ensure the most accurate results on samples of very high stiffness
• Multi-color status lights provide clear and visible indication of instrument and test status
• WinTest^® and TRIOS Software packages provide powerful and easy-to-use instrument control and data analysis for the ultimate flexibility in experimental design

Light or laser flash is a crucial measurement technique used to determine the thermal diffusivity, thermal conductivity, and specific heat capacity of materials. This method is useful in characterizing the heat transfer and storage properties of a variety of materials, providing essential information about material composition and structure. Light/Laser flash is the most effective method for measuring thermal diffusivity over a wide range of temperatures and offers non-destructive material testing with accurate, reproducible results. The Xenon and Laser Flash instruments generate high-energy Laser or Xenon pulse sources and use a PIN contact detector or non-contact IR detector to measure the resulting temperature rise. The selection of the ideal source and detector depends on various factors such as sample morphology, dimensions, expected thermal conductivity, and measurement temperature range.

TA Instruments Discovery Flash product line offers the most compelling range of benchtop and floor-standing flash diffusivity analyzers, enabling the analysis of a wide array of material forms and providing true measurements without the need for extrapolation. TA Instruments’ proprietary light flash technology, combined with full time pulse mapping, precision optics, and the latest data analysis models, make the Discovery Flash platform the most versatile, accurate and precise light flash system of its kind. It offers measurement capabilities over the broadest temperature range from -175°C up to 2800°C and multiple source and detector options. Additionally, a variety of sample holders and fixtures allow for in-plane measurement of thin-films, through-plane analysis of thick samples, and metals through their melt transition. Every system includes a multiple specimen autosampler that provides a several times increase in productivity and accuracy of specific heat capacity results. The Discovery Flash platform is an ideal choice for non-destructive material testing, providing reliable and reproducible results for a wide range of applications.